structural and morphology study of zno/cuo powders prepared by combination of sol-gel auto combustion and ultrasonic irradiation methods with different fuels

نویسندگان
چکیده

nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize zno/cuo nanocomposites. this method is based on the gelling and further combustion of solution in aqueous phase which contain salts of the desired metals and fuels. consequently, zno/cuo powders were prepared with molar ratio of nitrates to fuels 1:2. combustion process is inexpensive since it does not involve intermediate decomposition and/or calcining steps. combustion process ends, within 30 seconds for all systems.. finally, the product powder was characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem).

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Structural and Morphology Study of ZnO/CuO Powders Prepared by Combination of Sol-gel Auto Combustion and Ultrasonic Irradiation Methods with Different Fuels

Nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. Sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize ZnO/CuO nanocomposi...

متن کامل

Structural and Morphology Study of ZnO/CuO Powders Prepared by Combination of Sol-gel Auto Combustion and Ultrasonic Irradiation Methods with Different Fuels

Nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. Sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize ZnO/CuO nanocomposi...

متن کامل

Effect of pH on nanocrystalline Co-ferrite prepared using urea and thiourea fuels by combination of sol-gel auto combustion and ultrasonic irradiation methods

The aim of this study is to evaluate the influence of pH on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. Two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare CoFe2O4 powders. The morphology of the resulting powders was investigated. The powders wer...

متن کامل

Effect of pH on nanocrystalline Co-ferrite prepared using urea and thiourea fuels by combination of sol-gel auto combustion and ultrasonic irradiation methods

The aim of this study is to evaluate the influence of pH on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. Two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare CoFe2O4 powders. The morphology of the resulting powders was investigated. The powders wer...

متن کامل

effect of ph on nanocrystalline co-ferrite prepared using urea and thiourea fuels by combination of sol-gel auto combustion and ultrasonic irradiation methods

the aim of this study is to evaluate the influence of ph on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare cofe2o4 powders. the morphology of the resulting powders was investigated. the powders were characterized by x-r...

متن کامل

Preparation and Evaluation of NiFe204 and CuFe204 Nanoeatalysts by Combination of Sol- Gel Auto-Combustion Method and Irradiation Technique

The dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. Cu and Ni Unites nanocatalyst powders sithcomposition of Caned], and NiFe204 were synthesized by a sol-gel auto catalnic combustion process. Themolar ratio between metal ions and urea was 11.2. The sob gel process was done at 8...

متن کامل

منابع من

با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید


عنوان ژورنال:
international journal of bio-inorganic hybrid nanomaterials

جلد ۳، شماره ۳، صفحات ۱۶۳-۱۶۷

میزبانی شده توسط پلتفرم ابری doprax.com

copyright © 2015-2023